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A specific caution for copper peptides: heat, shaking and incompatible diluents can drive copper to dissociate from the peptide, and loosely bound Cu can generate reactive oxygen species another reason to keep handling gentle and cold [2]
In fact, the US Anti-Doping Authority says there is a concerning lack of published clinical trial data because studies appear to have been cancelled or stopped without any published conclusions
and Research, Certain Bulk Drug Substances for Use in Compounding that May Present Significant Safety Risks, FDA , Apr
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