Ketoprofen Micronized USP omega-Chloroalkanols 50% SOLUBILITY IN WATER TO

50% SOLUBILITY IN WATER TO PASS TEST TO PASS TEST ACIDITY 0

8 pH OF A 1 IN 100 SOLUTION 5

Test Specification Min Max APPEARANCE @ 25 Degrees C YELLOW LIQUID YELLOW LIQUID SAPONIFICATION VALUE 92 - 102 92 - 102 pH (5% IN WATER) 05-Jul 05-Jul ACID VALUE 10 COLOR (GARDNER) 5 MOISTURE 1

10% ELEMENTAL IMPURITIES AS REPORTED THIOCYANATE TO PASS TEST IDENTIFICATION TO PASS TEST RETEST DATE DATE OF MANUFACTURE APPEARANCE RESIDUAL SOLVENTS TO PASS TEST

Test Specification Min Max ASSAY 98% 98% MELTING RANGE 51 - 53 C 51 - 53 C

Ketoprofen Micronized USP omega-Chloroalkanols 50% SOLUBILITY IN WATER TOTest Specification Min Max ASSAY (DRIED BASIS) 98. 5 101. 00% MELTING RANGE 92. 0 97. 0 SPECIFIC ROTATION, [a][@D@]25 +1 to 1 +1 to 1 LOSS ON DRYING 0. 50% ORGANIC IMPURITIES TO PASS TEST TO PASS TEST RESIDUE OF IGNITION 0. 20% ELEMENTAL IMPURITIES AS REPORTED AS REPORTED IDENTIFICATION TO PASS TEST TO PASS TEST EXPIRATION DATE DATE OF MANUFACTURE APPEARANCE RESIDUAL SOLVENTS TO PASS TEST TO PASS TEST